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All published articles 1032

A Review on Nanotechnology: Analytical Techniques Use and Applications

Tassew Belete Bahru & Eyasu Gebrie Ajebe · International Research Journal of Pure and Applied Chemistry · 2019

The combination of nanotechnology with molecular biology, information technology and instrumentation, is opening the door to a new industrial age. The aim of this review article is to summarize the current knowledge of nanotechnology in synthesizing, identifying and characterizat...

Open access Research Article 10.9734/irjpac/2019/v19i430117

Experimental and Theoretical Evaluation of the Structure and Properties of New Stannyl Complexes of Pyridine Amide Ligands

Raji Thomas & Pushpa Pardasani · International Research Journal of Pure and Applied Chemistry · 2019

Aims: Penta and tetra coordinated stannyl derivatives of N, N'-Bis(2-pyridyl)pyridine-2,6-dicarboxamide (H2L) and N-(pyridine-2-yl)picolinamide (HL1) have been synthesized. The structure of the complexes has been well established by Sn119 NMR and computational studies (GAUSSIAN 0...

Open access Research Article 10.9734/irjpac/2019/v19i330112

Determination of Amlodipine Besilate and Azilsartan Medoxomil by UHPLC, HPTLC and Spectrophotometric Techniques

Marwa Mohammed Soliman, Manal Kamal Darwish & Sawsan Abdel-Moneem Abdel-Razeq · International Research Journal of Pure and Applied Chemistry · 2019

Aims: To develop methods with complete validation according to ICH guidelines and to be applied for the determination of both drugs in laboratory prepared mixtures and in synthetic tablets. Study Design:  Ultra high performance liquid chromatography (UHPLC), High performance thin...

Open access Research Article 10.9734/irjpac/2019/v19i330109

Evaluate the Effect of Processing of Chhattisgarh Local Paddy Variety to Flaked Rice (POHA) on Proximate, Chemical and Functional Characteristics

Rahul Dahare, Bhupendra Sahu & Tankesh Kumar · International Research Journal of Pure and Applied Chemistry · 2019

The present study was undertaken to study the evaluate the effect of processing of Chhattisgarh local paddy variety to flaked rice (Poha) on proximate, functional and chemical characteristics. In the proximate analysis, change in crude fat content from paddy 3.20% to 0.96% for th...

Open access Research Article 10.9734/irjpac/2019/v19i330110

Purification and Characterization of α-amylase from a Novel Thermoalkalophilic Strain of Bacillus sonorensis GV2 Isolated from Mushroom Compost

Gitanjali Vyas, Nivedita Sharma & Nisha Sharma · International Research Journal of Pure and Applied Chemistry · 2019

A novel thermoalkalophilic α-amylase producing bacterial strain Bacillus sonorensis GV2 |KJ775811.1| was isolated from mushroom compost. The purification of α-amylase was performed through different chromatography techniques. After purification with SDS-PAGE and Sephadex G-75 gel...

Open access Research Article 10.9734/irjpac/2019/v19i330111

Cyanuric Chloride / Manganese Chloride Tetrahydrate Catalyzed Beckmann Rearrangement of Ketoximes

Tong Shen-Yue, Lu Jue-Lin, Li Xiao-Wen, NI Wan-Min, Xu Ke-Wei & Feng Qi · International Research Journal of Pure and Applied Chemistry · 2019

In order to find an efficient catalytic system for Beckmann rearrangement of ketoximes, cyanuric chloride and Lewis acids were screened, and the cyanuric chloride /manganese chloride tetrahydrate system with good catalytic effect has been discovered. Using 2 mol% cyanuric chlorid...

Open access Research Article 10.9734/irjpac/2019/v19i230108

Synthesis, Physico-chemical and Antimicrobial Studies on Metal (II) Complexes with Schiff Base Derived from Salicylaldehyde and 2,4-Dinitrophenylhydrazine

H. Mukhtar, U. Sani & U. A. Shettima · International Research Journal of Pure and Applied Chemistry · 2019

Schiff base derived from salicylaldehyde and 2,4-dinitrophenylhydrazine was synthesized. Its Mn(II) and Fe(II) complexes (MnL2 and FeL2) were synthesized by refluxing the metal (II) chlorides with the Schiff base. All the compounds were characterized by melting point/decompositio...

Open access Research Article 10.9734/irjpac/2019/v19i230107

Health Risk Analysis of Heavy Metals (Cr, Fe, Hg & Ni) in Edible Vegetables in Yala Urban Area of Cross River State, Nigeria

Akpe, Michael Akomaye, Ashishie, Providence Beteluwhobel & Inezi, Faith Patrick · International Research Journal of Pure and Applied Chemistry · 2019

Aim: The aim of the study was to determine concentration of heavy metals in the soil and edible vegetables planted consumed Yala Urban Area of Cross River State, Nigeria, ascertained the level of metals contamination and the possible health risk or implication. Sampling: Forty ei...

Open access Research Article 10.9734/irjpac/2019/v19i230105

Characterization of Biochars and Their Application Rates on Soil Moisture Retention in Light Textured Soil of Assam

K. Deka, P. P. Hazarika, B. K. Medhi, Rupjyoti Borah, G. G. Kandali & Bhabesh Gogoi · International Research Journal of Pure and Applied Chemistry · 2019

“Biochar” is a relatively new term, yet it is not a new substance. Biochar, product of thermal decomposition or incomplete combustion of biomass or bio-wastes under limited oxygen supply, are fine-grained highly porous charcoal substances that are distinguished from other charcoa...

Open access Research Article 10.9734/irjpac/2019/v19i230106

Standardisation and Evaluation of Foxtail Millet Based Malt Mix

Jelang Jelku D. Sangma, W. Jessie Suneetha, B. Anila Kumari & K. B. Suneetha Devi · International Research Journal of Pure and Applied Chemistry · 2019

Foxtail millet has been consumed similar to rice from times immemorial and many products like soups, vermicelli, pasta and malt mixes were done in recent times to increase the nutrient content of various food products. Due to climate changes, millet usage is increasing nowadays a...

Open access Research Article 10.9734/irjpac/2019/v19i230104

Developed and Evaluation of Slow Release Phosphorus Fertilizer Using Mono-ammonium Phosphate and Di-ammonium Phosphate

Khalid Al Rohily, Adel Ghoneim, Hany El-Hamshary & Abdullah Modaihsh · International Research Journal of Pure and Applied Chemistry · 2019

Phosphorus (P) availability is generally low in Calcareous soils due to its association with soil constituents forming other P compounds that are of low solubility and availability for plant uptake. In particular, phosphorus use efficiency (PUE) in Saudi Arabia agricultural soils...

Open access Research Article 10.9734/irjpac/2019/v19i130103

Sustainable Bio-Adsorbent for Treatment of Nitrate, Fluoride and TDS in Groundwater

Anupam Singhal, Rajiv Gupta & Arun Singh · International Research Journal of Pure and Applied Chemistry · 2019

The quality of groundwater and surface water bodies have been analyzed globally and showed that 23% of primary drinking water sources have more than permissible limits of pollutants’ concentration. A major part of the world suffers from high concentrations of Nitrate, Fluoride an...

Open access Research Article 10.9734/irjpac/2019/v19i130102

Efficiency of Sawdust from Selected African Indigenous Wood spp. as a Low-cost Adsorbent for Removal of Copper Ion from Contaminated Water

E. A. Iyiola, J. M. Owoyemi, T. P. Saliu, B. Olufemi, D. O. Dania, O. Olasunkanmi, S. O. Ayanleye & A. Wekesa · International Research Journal of Pure and Applied Chemistry · 2019

Aims: This study investigates the use of sawdust from 3 hardwood species as low-cost adsorbent for the removal of copper from contaminated water. Study Design: The experimental design used for this study was 3 x 2 x 4 factorial experiment; the different sawdust species, two basel...

Open access Research Article 10.9734/irjpac/2019/v19i130101

Synthesis of Benzil by Air Oxidation of Benzoin and M(Salen) Catalyst

Qiuxin Shen, Liting Xu, Yiyan Jiang, Ran Zheng & Yiping Zhang · International Research Journal of Pure and Applied Chemistry · 2019

Bis salicylaldehyde ethylenediamine Schiff base (Salen) and its complexes with three metal ions (Co2+, Ni2+, Zn2+) were prepared, and characterized by infrared spectroscopy(IR). Using air as oxygen source, the optimum reaction conditions for the catalytic oxidation of 0.05 mol be...

Open access Research Article 10.9734/irjpac/2019/v19i130100

Determination of Antioxidant Activity of Leave Extracts of Albizia chevalieri Using Free Radical Scavenging Activity Assay

Alhassan M. Garba, Habiba R. Isa, Sadiq Abubakar & Saudat Ja’afar · International Research Journal of Pure and Applied Chemistry · 2019

Dried and powdered leaves of Albizia chevalieri were extracted using ethanol. The extract was fractionated to give methanol, chloroform and pet-ether. The four extracts obtained; ethanol, chloroform, methanol and pet-ether were evaluated for antioxidant activity using 2,2-dipheny...

Open access Research Article 10.9734/irjpac/2019/v19i130099