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All published articles 1032

Determination of Physico-Chemical Parameters, Zinc and Iron Levels in Domestic Waters of Katsina Metropolis, Nigeria

Lawal Shuaibu, Bashir Ahmed Dutsinma & Aliyu Ibrahim Yar’adua · International Research Journal of Pure and Applied Chemistry · 2014

Physico-chemical parameters, Zinc and Iron levels of sixteen different samples of the domestic waters obtained from some designated areas in Katsina metropolis were determined to ascertain the level of water quality. The parameters investigated were pH: (6.55±0.10-8.34±0.15), tur...

Open access Research Article 10.9734/IRJPAC/2015/13512

Evaluation of Heavy Metals in Road Dust in Jos, Plateau State, Nigeria

Temitope Ruth Alonge-Emmanuel, Fatai Afolabi Ayeni, Dorcas Joseph, Emily Dada & Florence Dennis Uzuh · International Research Journal of Pure and Applied Chemistry · 2014

An investigation of the heavy metal contents in road dust is vital in assessing the potential environmental impacts of vehicular emissions on the soil. In this study, dust samples were collected from Jos metropolis and were analysed for heavy metals (Pb, Zn, Mn, Cu, Co, Cd and Fe...

Open access Research Article 10.9734/IRJPAC/2015/14150

Level of Organochlorine Pesticides Residue in Fish, Water and Sediment in Biu Dam (Reservoir) Borno State Nigeria

D. Y. Shinggu, O. N. Maitera & J. T. Barminas · International Research Journal of Pure and Applied Chemistry · 2014

The health risks posed by organochlorine compounds to the total environment have continued to elicit concern among researchers in developing countries worldwide. Hence, this study focused on investigating the levels of Organochlorine pesticides residues in water sediment and fish...

Open access Research Article 10.9734/IRJPAC/2015/13199

Optimization and Kinetic Study for the Removal of Chromium (VI) Ions by Acid Treated Sawdust Chitosan Composite Beads

N. M. I. Alhaji & K. M. Tajun Meera Begum · International Research Journal of Pure and Applied Chemistry · 2014

Aims: To study the adsorption efficiency of acid-treated sawdust composite beads (SDCCB) for Cr(VI) ions and to optimize the process variables using Response Surface Methodology (RSM). Study Design: Preparation of SDCCB, Characterization of SDCCB, Study of influence of variables...

Open access Research Article 10.9734/IRJPAC/2015/13834

Kinetics and Mechanism of the Reaction of Malachite Green and Dithionite Ion

S. O. Idris, A. Tanimu, J. F. Iyun & Y. Mohammed · International Research Journal of Pure and Applied Chemistry · 2014

The kinetics of the oxidation of malachite green, MG+, by dithionite ions, S2O42- have been studied spectrophotometrically in an aqueous acid free medium. The investigation was carried out under pseudo- first order conditions of an excess of dithionite concentration. Reaction con...

Open access Research Article 10.9734/IRJPAC/2015/12428

Measuring the Electrochemical Response of a Titanium Dioxide Nanotube Electrode to Various Chemicals as Explosive Components

Samuel C. Johnson, Yong X. Gan, Sinclair B. Calderon, James L. Smith & Jimmie C. Oxley · International Research Journal of Pure and Applied Chemistry · 2014

Sensing and mitigating explosives are critical for homeland security. This paper investigates the electrochemical responses of TiO2 nanotubes exposed to several chemicals including ammonium nitrate, hydrogen peroxide, methanol, ethanol and ethylene glycol which are used directly...

Open access Research Article 10.9734/IRJPAC/2015/14263

Crystallographic and Structural Analysis of Heterometallic FeAg Complexes

M. Melník & P. Mikuš · International Research Journal of Pure and Applied Chemistry · 2014

There are 30 heterometallic Fe/Ag complexes in this review. The complexes contain the following metallic cores: FeAg, Fe2Ag, FeAg2, FeAgW, Fe2Ag2, FeAg3, Fe4Ag, Fe3Ag2, Fe2Ag4, Fe2Ag2Pd2, Fe6Ag, Fe4Ag4, Fe4Ag5, Fe3Ag6 and {FeAg}n. The mean M-M bond distance elongated in the order...

Open access Research Article 10.9734/IRJPAC/2015/13420

Delayed Shifts in pH Responses to Weak Acids in Spring Water Exposed to Circular Rotating Magnetic Fields: A Narrow Band Intensity-Dependence

Nirosha J. Murugan, Lukasz M. Karbowski, Blake T. Dotta & Michael A. Persinger · International Research Journal of Pure and Applied Chemistry · 2014

The time required for the shift in pH after addition of small quantities of a weak acid into fixed volumes of spring water was measured once per minute while the sample was exposed to magnetic field configurations that have been shown to influence photon emissions and to produce...

Open access Research Article 10.9734/IRJPAC/2015/13156

Synthesis and Characterization of Impurities of a Common and Advanced Intermediate of Candesartan and Azilsartan Antihypertensive Drugs

Sangeeta Sangwan, Tapas Panda, Kaushal Nayyar, Sharwan K. Dewan & Rajesh K. Thaper · International Research Journal of Pure and Applied Chemistry · 2014

Six impurities were identified in the lab development batches during the course of benzimidazole intermediate (1) synthesis by reverse phase HPLC method. Intermediate 1 is used as a common and advanced intermediate in the synthesis of candesartan and azilsartan. All the impuritie...

Open access Research Article 10.9734/IRJPAC/2015/13162

Determination of Nitrogen and Sulphur Oxides Produced During Combustion of the Jatropha Cake as a Measure of the Level of Pollution When the Cake is Used as a Fuel

S. Mbera, L. R. M. Nhamo & T. Nyakungu · International Research Journal of Pure and Applied Chemistry · 2014

Jatropha cake is a promising renewable energy source after proving difficult to be used as feedstock. Its possible use as a combustible fuel makes the Jatropha cake pellet important as a source of potentially harmful gases to the users and the environment. This makes it imperativ...

Open access Research Article 10.9734/IRJPAC/2015/12889

Liquid Laundry Detergents Based on Novel Polymeric Surfactants

A. G. Deshmukh, B. B. Gogte & M. K. N. Yenkie · International Research Journal of Pure and Applied Chemistry · 2014

A novel polymer based on sorbitol, polyethylene glycol, citric acid has been synthesized using HCl as catalyst. The experimental conditions, order of addition of ingredients, ratio of ingredients, catalyst, time and temperature have been standardized to get desired molecular weig...

Open access Research Article 10.9734/IRJPAC/2015/12459

Comparisons between Polyvinyl Alcohol (PVOH) and Sodium Dodecyl Sulphate (SDS) as Surfactants in Natural Rubber (NR)/Polyvinyl Acetate (PVAc) Latex Blends

Stephen Shaibu Ochigbo & Mohammed Abubakar Tanko Suleiman · International Research Journal of Pure and Applied Chemistry · 2014

Solutions of sodium dodecyl sulphate (SDS) and polyvinyl alcohol (PVOH) were used respectively as surfactants in comparative viscosity measurements of pure polyvinyl acetate (PVAc) emulsion, natural rubber (NR) latex and their blends using Ostwald glass capillary viscometer. Resu...

Open access Research Article 10.9734/IRJPAC/2015/7688

Synthesis of Nitrogen-Containing Chalcone Via One-Pot Three-Component Reaction: Part IV

Anwar E. M. Nor-Eljaleel, Himat M. A. Fadul, Saad M. H. Ayuob, M. Abdel Karim, Jan H. van der Westhuizen & M. J. A. Abualreish · International Research Journal of Pure and Applied Chemistry · 2014

The mannich reaction is one of the most important C-C bond formation methods in organic   synthesis. The mannich-reaction is employed in the   organic synthesis of natural compounds like for instance peptides-nucleotides-antibiotics and alkaloids. Other application are in agroche...

Open access Research Article 10.9734/IRJPAC/2015/13111

Crystallographic and Structural Analysis of Heterometallic FeCu Complexes

M. Melník & P. Mikuš · International Research Journal of Pure and Applied Chemistry · 2014

Over 100 heterometallic FeCu complexes, from heterodi- to heteropolymeric have been included in this review. The complexes contain the FeCu, Fe2Cu, FeCu2, FeCuMo; Fe3Cu, Fe2Cu2, Fe2CuM (M=Hg or Co); Fe4Cu, Fe3CuTe; Fe4Cu2, Fe3Cu3; FeCu6, FeCu2Ru4; Fe4Cu4, Fe4Cu5; Fe6Cu5 and {FeCu...

Open access Research Article 10.9734/IRJPAC/2015/12290

Assessment of the Phytochemical, Proximate, Vitamin and Mineral Composition of Solanum gilo L.

Sunday Onykwere Eze & Chidinma Queeneth Kanu · International Research Journal of Pure and Applied Chemistry · 2014

Assessment of the phytochemical, proximate, vitamins and mineral composition of S. gilo L was undertaken using standard methods. The phytochemical screening revealed that the plant contained tannins, saponins, phenols, cyanogenic glycosides, alkaloids and flavonoids, The results...

Open access Research Article 10.9734/IRJPAC/2015/12484