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All published articles 1032

Synthesis, Characterization and Metal Picrate Extraction Studies of Salicylaldehyde Derived Macrocyclic Schiff Bases

Misbah Ur Rehman, M. Imran, M. Arif & M. Farooq · International Research Journal of Pure and Applied Chemistry · 2014

Three novel Salicylaldehyde derived macrocyclic Schiff bases were synthesized and well characterized by Elemental analyses, IR, Mass and 1HNMR spectral data. The liquid-liquid extraction of metal cations (Ag+ and Cu2+) from aqueous phase to organic phase was carried out using the...

Open access Research Article 10.9734/IRJPAC/2014/8147

Preparation of Macroporous Poly (GMA-DVB) and Its Application to Immobilize β-Galactosidase from Aspergillus Oryzae

Sun Sufang, Ming Xuejie & PengLulu . · International Research Journal of Pure and Applied Chemistry · 2013

The reactive, macroporous glycidyl methacrylate (GMA) and divinyl benzene (DVB) polymer was synthesized with a mixture of cyclohexanol and lauryl alcohol as liquid pore-forming agents and nano-calcium carbonate as solid one via suspension polymerization. The surface structure of...

Open access Research Article 10.9734/IRJPAC/2014/7241

Study of Molecular Interactions in Ternary Mixtures of Quinoline with o-cresol, m-cresol and p-cresol in Methanol at T= 303.15, 308.15, 313.15, and 318.15 K

Ch. Kavitha, A. Ratnakar, M. Durga Bhavani & K. Narendra · International Research Journal of Pure and Applied Chemistry · 2013

Aims: To evaluate the thermodynamical parameters and their excess functions to find the molecular interactions between unlike molecules in ternary liquid mixtures. Study Design: Ultrasonic velocities, densities and viscosities have been measured for the ternary mixtures of quinol...

Open access Research Article 10.9734/IRJPAC/2014/6636

Bio-ethanol Production from Thermally Pre-treated Corn Chaff and Cassava Waste Water

C. N. Ibeto, C. O. B. Okoye & A. U. Ofoefule · International Research Journal of Pure and Applied Chemistry · 2013

The production of bio-ethanol from corn chaff and cassava waste water was carried out after pretreatment with liquid hot water. Proximate analysis was carried out on the wastes using standard methods and the results obtained for corn chaff were carbohydrate (1.64%), fibre (22%),...

Open access Research Article 10.9734/IRJPAC/2014/6913

Manganese and Magnesium Status of Forage Grasses, and It’s Implications for Grazing Animals, Dareta Village, Zamfara, Nigeria

U. U. Udiba, M. O. Odey, A. H. Jibril, Balli Gauje, Olaoye Sikemi, A. M. Sule, H. A. Mohammed & Mahmud Abdullahi · International Research Journal of Pure and Applied Chemistry · 2013

Forage mineral concentration is of considerable importance to livestock production. High concentrations of lead in the soil environment causes imbalance of mineral nutrients in growing plants. In most cases lead blocks the entry of cations (potassium, Calcium, Magnesium, Manganes...

Open access Research Article 10.9734/IRJPAC/2014/6258

Reduction Kinetics of 3,7-bis (dimethylamino)-4-nitro-phenothiazine-5-ium Chloride (Methyelene Green) with Potassium Persufate in Presence of Halides

Rehana Saeed, Fahim Uddin, Maria Ashfaq, Muna Irfan & Zahida Khalid · International Research Journal of Pure and Applied Chemistry · 2013

The effect of ionic strength and temperature on the kinetics of reaction between 3, 7 bis (dimethyl amino) - 4- nitro-phenothiazine-5-ium chloride (methylene green) and persulfate ions in presence of potassium iodide and potassium bromide was studied by spectrophotometric method....

Open access Research Article 10.9734/IRJPAC/2014/6649

Application of Newton’s Zero Order Caustic for Analysis and Measurement: Part III – Light Scattering

Antonio A. Garcia, Luis Nuñez, Angel Lastra Miranda & Vladimiro Mujica · International Research Journal of Pure and Applied Chemistry · 2013

When light is incident upon a liquid suspension that has an oblate spheroid shape, the size and presence of particles can be determined by measuring light intensity exiting the sample or by imaging the scattered light using a digital camera. This dual analysis system is facilitat...

Open access Research Article 10.9734/IRJPAC/2014/5899

Synthesis and Single Crystal XRD of Hydroniumpentaaquabis(1,10-phenanthroline) europium(III)tetrachloride Hydrate [(H3O+)(H2O)5(phen)2Eu(III)]Cl4.H2O

Sudalaiandi Kumaresan · International Research Journal of Pure and Applied Chemistry · 2013

A novel europium(III)-1,10-phen complex (I) has been synthesized and characterized by single crystal XRD. Complex I crystallized in the monoclinic space group C2/c with unit cell dimensions a = 30.8233(13) Å, b = 9.5063(4) Å, c = 21.9973(10) Å, α = 90°, β = 113.616(2)°, γ = 90°,...

Open access Research Article 10.9734/IRJPAC/2014/6646

Morphology and Transport Properties of Polyethylene Oxide (PEO)-based Nanocomposite Polymer Electrolytes

T. O. Ahmed, P. O. Akusu, A. Ismaila & A. Maryam · International Research Journal of Pure and Applied Chemistry · 2013

Magnesium Oxide (MgO) Nanoparticles (Nps) synthesized by microwave-assisted coprecipitation method was added as a nanoscale filler together with sodium thiocyanate (NaSCN) into poly (ethylene oxide) (PEO) to form PEO-MgO/NaSCN Nanocomposite Polymer Electrolytes (NCPEs). The MgO N...

Open access Research Article 10.9734/IRJPAC/2014/5358

Development of a New Eco-Friendly Validated UV Spectrophotometric Method for Quantitative Determination of Acetaminophen in Tablet Dosage Form

Swati Jain, Ashutosh Pareek, Sarita singh, Pratima ., Sangeeta Kumari, Seema Verma, Vivek Jain & Yashumati Ratan · International Research Journal of Pure and Applied Chemistry · 2013

Aims: The present study was undertaken to develop a new UV spectroscopic method of acetaminophen using mix solution of methanol: phosphate buffer 7.4 (in 1:9 ratio) (further diluted with phosphate buffer 7.4 only) as a solvent system for analysis of acetaminophen. Place and Durat...

Open access Research Article 10.9734/IRJPAC/2014/5784

Determination of Saponin Content of Various Parts of Six Citrus species

Chinelo A. Ezeabara, C. U. Okeke, Bibian O. Aziagba, Chinyere V. Ilodibia & Adaeze N. Emeka · International Research Journal of Pure and Applied Chemistry · 2013

Different parts of Citrus aurantifolia (Christm.) Swingle (Lime), C. grandis Osbeck (Shaddock/Pummelo), C. limon (L.) Burm. f. (Lemon), C. paradisii Macf. (Grapefruit), C. reticulata Blanco (Mandarin/Tangerine) and C. sinensis (L.) Osbeck (Sweet orange) commonly cultivated in Sou...

Open access Research Article 10.9734/IRJPAC/2014/5831

Adsorption Characteristics of Sodium Oleate onto Calcite

I. J. Alinnor & C. K. Enenebeaku · International Research Journal of Pure and Applied Chemistry · 2013

Aims: The need for separation of calcite from other minerals has been a concern. Na-oleate has been found useful as a good adsorbate for separation of calcite from other minerals. The aim of present study is to investigate the effect of various mechanisms of adsorption of Na-olea...

Open access Research Article 10.9734/IRJPAC/2014/3555

Effect of Growth Temperature on Chemical Synthesis of PbS quantum dots

P. K. Kalita, B. Das & R. Devi · International Research Journal of Pure and Applied Chemistry · 2013

PbS quantum dots synthesized at room temperature through CBD technique show a large blue shift of absorption edge due to formation of very small particle size of the order of 2nm confirmed by HRTEM measurement. It exhibits a further blue shift when synthesized in acidic medium (p...

Open access Research Article 10.9734/IRJPAC/2014/5502

Determination of Optimum Reaction Temperature and Reaction Time for Biodiesel Yield from Coconut (Cocos nucifera) Oil

A. U. Ofoefule, C. N. Ibeto, L. C. Ugwu & D. C. Eze · International Research Journal of Pure and Applied Chemistry · 2013

The determination of optimum reaction temperature and time for biodiesel yield from Coconut (Cocos nucifera) oil was studied. The oil was transesterified using potassium hydroxide (KOH) in methanol as catalyst to obtain the crude biodiesel. For the reaction time, the biodiesel pr...

Open access Research Article 10.9734/IRJPAC/2014/3927

Zirconium (IV) Molybdo Tungstate- Application as Catalyst for the Synthesis of an Ester

H. K. Sharma & N. Sharma · International Research Journal of Pure and Applied Chemistry · 2013

Aims: The research work is based on the kinetic study of the esterification reaction of benzoic acid with alcohol by using zirconium molybdo tungstate and conventional catalyst (sulphuric acid). Study Design: The study was designed to compare the results of both the catalysts und...

Open access Research Article 10.9734/IRJPAC/2014/4347