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Research Article Open access CC BY 4.0

Synthesis and FTIR Analysis of Cd Doped Nano Ni - Aluminates

Ammara Yaseen, Adnan Yasin, Akasha Saleem, Faqeer Muhammad, Rafia Ismail, Muhammad Ismaeel, Ihsan Ali, Zarwali Khan, Muhammad Usman, Muhammad Ramzan, Tayyaba Shabir, Zobia Yaseen, Nasir Abbas

Asian Journal of Chemical Sciences · pp. 57–70 · Published 15 Sep 2023

10.9734/ajocs/2023/v13i5253

Abstract

Nano Ni – Aluminates (Ni0.5 Fe0.5 Al2O4) and Cd Doped Nano Ni – Aluminates (Ni0.5 Fe0.5 Al2-x CdxO4) where x = 0.2, 0.4, 0.6 and 0.8 were synthesized by co-precipitation method. Ammonium hydroxide was used as precipitating agent. The samples were characterized using Fourier transform infrared spectroscopy.  FTIR spectrum for each unannealed sample of Ni0.5 Fe0.5 Al2 O4 and Ni0.5 Fe0.5 Al2-x Cdx O4 exhibit a broad band near 3450 cm-1 due to –OH stretching vibration of free hydrogen bonded hydroxyl group and a second typical absorption band at 1620 cm-1 resulting from deformative vibration of water molecules. Spectra for samples after annealing show peaks in the range of 900-450 cm-1 and 850-500 cm-1    showing presence of Al-O and Ni-O bonds respectively thus confirm the formation of metal oxides bonds while no peak was observed for –OH bond. A peak around 420 cm-1 is assigned to Cd-O bond.

Nano-ni aluminates Cd doped nano ni-aluminates co-precipitation fourier transform infrared spectroscopy

References (37)

  1. 1 The Proceedings of the National Academy of Sciences [DOI]
  2. 2 Metal oxide nanoparticles and their applications in nanotechnology [DOI]
  3. 3 Nanotechnology Applications in Cancer [DOI]
  4. 4 Detail review on chemical, physical and green synthesis, classification, characterizations and applications of nanoparticles [DOI]
  5. 5 Making polymeric micro- and nanoparticles of complex shapes [DOI]
  6. 6 Metal‐Based Nanomaterials in Biomedical Applications: Antimicrobial Activity and Cytotoxicity Aspects [DOI]
  7. 7 3D printed functional nanomaterials for electrochemical energy storage [DOI]
  8. 8 Emergent Pseudocapacitance of 2D Nanomaterials [DOI]
  9. 9 Optical Properties of (Oxy)Nitride Materials: A Review [DOI]
  10. 10 Scanning Electron Microscopy: Principle and Applications in Nanomaterials Characterization [DOI]
  11. 11 Methods of Chemical Synthesis in the Synthesis of Nanomaterial and Nanoparticles by the Chemical Deposition Method: A Review [DOI]
  12. 12 Novel applications of solid and liquid formulations of nanoparticles against insect pests and pathogens [DOI]
  13. 13 Nanomaterials properties [DOI]
  14. 14 Cation Distribution in Spinel Ferrite Nanocrystals: Characterization, Impact on their Physical Properties, and Opportunities for Synthetic Control [DOI]
  15. 15 Quantum chemical design of nonlinear optical materials by sp2-hybridized carbon nanomaterials: issues and opportunities [DOI]
  16. 16 Applied dental materials [DOI]
  17. 17 Photobiology in protected horticulture [DOI]
  18. 18 Clay-Supported Metal Oxide Nanoparticles in Catalytic Advanced Oxidation Processes: A Review [DOI]
  19. 19 General Synthesis of Porous Mixed Metal Oxide Hollow Spheres with Enhanced Supercapacitive Properties [DOI]
  20. 20 Applications of Metal/Mixed Metal Oxides as Photocatalyst: A Review [DOI]
  21. 21 Designer Nanomaterials through Programmable Assembly [DOI]
  22. 22 One-dimensional nanomaterials for energy storage [DOI]
  23. 23 Types and classification of nanomaterials [DOI]
  24. 24 Template Synthesis of Nanoparticle Arrays of Gold and Platinum in Mesoporous Silica Films [DOI]
  25. 25 Electrochemical fabrication of single-crystalline and polycrystalline Au nanowires: the influence of deposition parameters [DOI]
  26. 26 Magnetic Spinels - Synthesis, Properties and Applications [DOI]
  27. 27 Fabrication and nonlinear optical investigations of SiO 2 @Ag core-shell nanoparticles [DOI]
  28. 28 Synthesis and Characterization of Nano-Sized Nickel Aluminate Spinel Crystals [DOI]
  29. 29 Structural and Thermodynamic Variation in Nickel Aluminate Spinel [DOI]
  30. 30 Designer Nanomaterials through Programmable Assembly [DOI]
  31. 31 Structural defects in AFe2O4 (A=Zn, Mg) spinels [DOI]
  32. 32 Nature of Magnetic Ordering in Cobalt‐Based Spinels [DOI]
  33. 33 Nanotechnology: Trends and Future Applications [DOI]
  34. 34 Structural, Optical, Magnetic, and Electrical Properties of Ni0.5Co0.5Al2O4 System [DOI]
  35. 35 Morphology of nickel aluminate spinel (NiAl2O4) formed in the Al2O3-Ni composite system sintered in air
  36. 36 Introduction: 1D Nanomaterials/Nanowires [DOI]
  37. 37 Nanotechnology: The New Features [DOI]

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